Makatite Annehed H, Faelth L, Lincoln F J Zeitschrift fur Kristallographie 159 (1982) 203-210 Crystal structure of synthetic makatite Na2Si4O8(OH)2(H2O)4 _database_code_amcsd 0010848 CELL PARAMETERS: 7.3881 18.0940 9.5234 90.000 90.640 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1273.011 Density (g/cm3): 2.082 MAX. ABS. INTENSITY / VOLUME**2: 5.387796890 RIR: 0.843 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.78 51.92 9.0470 0 2 0 2 10.50 26.11 8.4270 0 1 1 4 17.40 100.00 5.0953 0 3 1 4 18.16 3.84 4.8862 1 2 1 4 18.64 4.03 4.7614 0 0 2 2 19.00 1.43 4.6721 1 3 0 4 19.63 4.20 4.5235 0 4 0 2 21.08 16.80 4.2135 0 2 2 4 21.12 3.07 4.2062 -1 3 1 4 22.33 2.22 3.9820 1 0 2 2 22.64 6.73 3.9268 -1 1 2 4 22.87 7.40 3.8889 1 1 2 4 23.05 7.77 3.8578 1 4 0 4 23.81 22.43 3.7372 0 3 2 4 24.09 69.86 3.6938 2 0 0 2 24.21 5.22 3.6757 -1 2 2 4 24.60 1.49 3.6192 2 1 0 4 24.85 5.79 3.5828 -1 4 1 4 26.06 64.88 3.4198 2 2 0 4 26.25 4.32 3.3954 -2 1 1 4 26.35 15.22 3.3828 0 5 1 4 26.44 3.52 3.3709 2 1 1 4 26.64 1.09 3.3466 -1 3 2 4 26.83 1.75 3.3231 1 3 2 4 27.19 9.85 3.2795 0 4 2 4 27.62 1.41 3.2292 -2 2 1 4 27.81 2.97 3.2080 2 2 1 4 28.55 33.26 3.1265 0 1 3 4 29.62 5.46 3.0157 0 6 0 2 29.83 40.06 2.9953 0 2 3 4 29.89 3.27 2.9889 1 4 2 4 30.46 2.01 2.9345 -2 0 2 2 30.80 1.76 2.9029 2 0 2 2 30.93 2.79 2.8907 -1 1 3 4 31.04 23.69 2.8811 0 5 2 4 31.11 13.54 2.8750 0 6 1 4 31.19 1.13 2.8680 1 1 3 4 31.26 4.49 2.8611 2 4 0 4 32.06 5.78 2.7920 1 6 0 4 32.07 6.33 2.7913 -2 2 2 4 32.13 2.03 2.7860 -1 2 3 4 32.39 5.72 2.7641 2 2 2 4 33.30 2.83 2.6904 -1 5 2 4 33.41 1.01 2.6823 -1 6 1 4 33.48 3.47 2.6762 1 6 1 4 33.97 1.34 2.6387 -2 3 2 4 34.03 1.62 2.6343 -1 3 3 4 35.23 15.37 2.5477 0 6 2 4 35.93 17.62 2.4997 -2 5 1 4 36.07 17.34 2.4898 2 5 1 4 36.77 3.12 2.4442 1 4 3 4 37.48 1.07 2.3995 -2 1 3 4 37.70 1.54 2.3863 0 5 3 4 37.79 5.08 2.3807 0 0 4 2 37.91 1.56 2.3736 2 1 3 4 37.97 4.86 2.3700 -3 1 1 4 38.04 2.37 2.3656 -1 7 1 4 38.11 1.60 2.3614 1 7 1 4 38.13 11.71 2.3604 0 1 4 4 38.54 7.41 2.3360 2 6 0 4 38.97 1.34 2.3113 -3 2 1 4 39.54 5.46 2.2793 -2 5 2 4 39.81 4.31 2.2644 2 5 2 4 40.14 1.18 2.2466 -2 3 3 4 40.24 1.39 2.2412 1 1 4 4 40.54 1.43 2.2253 2 3 3 4 40.59 2.29 2.2224 -3 3 1 4 41.29 1.86 2.1863 0 6 3 4 41.76 1.50 2.1628 3 4 0 4 41.77 1.22 2.1627 1 8 0 4 42.33 1.13 2.1353 -3 2 2 4 42.93 4.27 2.1067 0 4 4 4 43.01 1.92 2.1031 -2 6 2 4 43.25 1.46 2.0921 1 6 3 4 43.26 3.09 2.0914 2 6 2 4 44.22 3.10 2.0480 3 3 2 4 45.06 1.14 2.0121 -2 5 3 4 45.37 1.51 1.9990 -2 1 4 4 45.42 1.31 1.9968 2 5 3 4 45.65 1.14 1.9871 3 5 1 4 45.85 1.04 1.9790 2 1 4 4 46.24 5.21 1.9634 -2 2 4 4 46.27 2.34 1.9620 3 4 2 4 46.72 4.83 1.9445 2 2 4 4 47.12 4.71 1.9289 2 8 0 4 47.68 5.27 1.9074 3 6 0 4 48.03 5.96 1.8941 0 1 5 4 48.20 2.76 1.8878 -2 6 3 4 48.55 3.27 1.8751 2 6 3 4 48.77 1.12 1.8671 3 6 1 4 49.34 14.16 1.8469 4 0 0 2 49.48 2.67 1.8420 0 8 3 4 49.60 1.27 1.8379 -2 4 4 4 50.05 2.24 1.8223 2 4 4 4 50.44 1.51 1.8094 0 10 0 2 51.02 2.21 1.7900 -1 8 3 4 51.35 2.69 1.7793 3 4 3 4 51.40 5.65 1.7776 0 10 1 4 51.70 2.86 1.7680 -1 3 5 4 51.74 1.58 1.7669 -2 7 3 4 52.04 1.16 1.7575 1 10 0 4 52.28 1.45 1.7499 3 7 1 4 52.61 1.70 1.7397 -4 3 1 4 52.83 1.05 1.7330 4 3 1 4 53.60 1.85 1.7099 4 4 0 4 54.44 2.64 1.6854 0 5 5 4 54.63 1.39 1.6799 4 4 1 4 54.70 1.02 1.6779 2 1 5 4 54.84 1.16 1.6742 -3 7 2 4 54.87 4.31 1.6733 -2 6 4 4 55.29 4.59 1.6615 2 6 4 4 55.97 1.11 1.6430 -3 8 1 4 56.09 1.13 1.6397 1 5 5 4 56.69 1.64 1.6238 -4 5 1 4 56.80 2.10 1.6209 0 11 1 4 56.90 1.31 1.6183 4 5 1 4 57.04 1.07 1.6146 -4 4 2 4 57.69 1.93 1.5979 -4 1 3 4 58.30 2.11 1.5826 4 1 3 4 58.37 3.32 1.5811 0 1 6 4 59.25 1.19 1.5597 -4 5 2 4 59.39 1.39 1.5563 -4 6 1 4 59.45 3.64 1.5547 0 11 2 4 59.65 1.70 1.5501 4 5 2 4 60.12 1.39 1.5391 -2 5 5 4 60.37 2.37 1.5333 0 7 5 4 61.58 1.13 1.5060 -1 9 4 4 61.96 1.38 1.4976 0 4 6 4 62.72 1.23 1.4813 -2 6 5 4 62.80 2.84 1.4796 -3 8 3 4 63.21 1.44 1.4711 2 6 5 4 63.84 1.18 1.4581 3 10 0 4 63.90 2.19 1.4568 0 8 5 4 64.27 1.52 1.4493 -2 10 3 4 64.56 1.63 1.4435 2 10 3 4 64.71 2.19 1.4406 0 10 4 4 64.86 2.06 1.4375 0 12 2 4 65.00 1.28 1.4349 -2 11 2 4 65.19 1.37 1.4311 2 11 2 4 66.58 1.25 1.4045 5 4 0 4 66.58 1.91 1.4045 0 6 6 4 66.69 2.01 1.4025 5 1 2 4 66.90 1.06 1.3986 -5 2 2 4 67.78 1.42 1.3826 0 9 5 4 67.81 1.26 1.3821 -2 12 1 4 71.04 1.30 1.3268 5 6 0 4 72.56 2.31 1.3028 0 4 7 4 72.85 1.39 1.2984 -2 9 5 4 73.30 1.38 1.2915 2 9 5 4 76.53 1.25 1.2449 0 11 5 4 77.42 1.02 1.2327 -2 4 7 4 78.60 1.21 1.2171 4 11 1 4 80.19 1.52 1.1970 0 14 3 4 81.39 1.09 1.1823 -2 11 5 4 83.63 1.31 1.1562 -5 8 3 4 84.00 1.63 1.1522 -5 3 5 4 85.83 1.27 1.1322 4 10 4 4 85.95 1.26 1.1309 0 16 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.