Pierrotite Engel P, Gostojic M, Nowacki W Zeitschrift fur Kristallographie 165 (1983) 209-215 The crystal structure of pierrotite, Tl2(Sb,As)10S16 Locality: Jas-Roux, Hutes-Alps, France _database_code_amcsd 0010859 CELL PARAMETERS: 38.7460 8.8160 7.9890 90.000 90.000 90.000 SPACE GROUP: Pna2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2728.920 Density (g/cm3): 4.751 MAX. ABS. INTENSITY / VOLUME**2: 32.75927761 RIR: 2.245 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 4.56 1.87 19.3730 2 0 0 2 9.13 5.27 9.6865 4 0 0 2 10.29 6.03 8.5963 1 1 0 4 11.98 1.36 7.3857 2 0 1 2 13.58 1.33 6.5199 4 1 0 4 14.37 2.72 6.1632 4 0 1 2 14.97 2.39 5.9199 0 1 1 2 15.14 5.09 5.8520 1 1 1 4 15.22 1.58 5.8203 5 1 0 4 15.65 5.86 5.6615 2 1 1 4 17.02 2.29 5.2096 6 1 0 4 17.66 3.72 5.0221 6 0 1 2 18.86 20.83 4.7043 5 1 1 4 18.93 1.66 4.6878 7 1 0 4 20.28 1.06 4.3797 1 2 0 4 20.35 2.90 4.3638 6 1 1 4 20.67 11.68 4.2981 2 2 0 4 20.93 14.47 4.2449 8 1 0 4 21.30 10.00 4.1717 3 2 0 4 21.46 9.14 4.1416 8 0 1 2 21.98 2.02 4.0431 7 1 1 4 22.26 40.20 3.9945 0 0 2 1 22.73 9.18 3.9122 2 0 2 2 22.99 8.39 3.8685 9 1 0 4 23.16 2.08 3.8405 1 2 1 4 23.50 17.17 3.7851 2 2 1 4 23.74 4.56 3.7486 8 1 1 4 24.07 1.99 3.6979 3 2 1 4 24.10 28.75 3.6928 4 0 2 2 24.45 24.42 3.6407 6 2 0 4 24.57 4.15 3.6225 1 1 2 4 24.83 100.00 3.5854 4 2 1 4 24.90 2.28 3.5759 2 1 2 4 25.55 79.79 3.4862 10 0 1 2 25.58 11.47 3.4818 9 1 1 4 25.79 2.48 3.4547 5 2 1 4 25.84 1.07 3.4482 7 2 0 4 26.16 5.94 3.4061 4 1 2 4 26.23 10.11 3.3971 6 0 2 2 26.91 6.39 3.3129 6 2 1 4 27.07 1.04 3.2935 5 1 2 4 27.26 5.43 3.2709 11 1 0 4 27.63 3.69 3.2288 12 0 0 2 28.19 8.13 3.1659 7 2 1 4 28.97 27.14 3.0816 8 0 2 2 29.46 1.04 3.0319 12 1 0 4 29.51 6.52 3.0271 11 1 1 4 29.60 40.01 3.0183 8 2 1 4 29.85 1.73 2.9936 12 0 1 2 30.19 11.03 2.9600 0 2 2 2 30.28 2.90 2.9514 1 2 2 4 30.51 2.76 2.9303 1 3 0 4 30.55 4.80 2.9260 2 2 2 4 30.74 2.09 2.9090 8 1 2 4 30.77 1.25 2.9054 2 3 0 4 31.00 1.50 2.8852 3 2 2 4 31.12 1.31 2.8737 9 2 1 4 31.56 9.37 2.8346 12 1 1 4 31.61 64.23 2.8307 4 2 2 4 32.19 9.26 2.7812 10 0 2 2 32.21 7.14 2.7789 9 1 2 4 32.35 1.25 2.7676 14 0 0 2 32.38 3.33 2.7651 5 2 2 4 32.46 8.94 2.7580 0 3 1 2 32.55 6.80 2.7510 1 3 1 4 32.75 1.38 2.7344 10 2 1 4 33.22 10.09 2.6972 3 3 1 4 33.30 72.17 2.6908 6 2 2 4 33.50 2.11 2.6747 6 3 0 4 33.67 5.04 2.6621 13 1 1 4 33.79 1.83 2.6523 10 1 2 4 33.98 3.63 2.6382 2 0 3 2 34.29 15.07 2.6151 14 0 1 2 34.47 2.42 2.6017 11 2 1 4 34.52 3.33 2.5983 5 3 1 4 34.94 5.52 2.5677 4 0 3 2 35.39 1.42 2.5364 6 3 1 4 35.47 2.38 2.5307 11 1 2 4 35.52 2.17 2.5275 2 1 3 4 35.54 9.95 2.5256 8 2 2 4 35.76 3.04 2.5111 12 0 2 2 35.82 5.88 2.5071 14 1 1 4 36.24 6.37 2.4789 15 1 0 4 36.27 1.67 2.4765 12 2 1 4 36.45 1.02 2.4653 4 1 3 4 36.50 8.50 2.4619 6 0 3 2 36.85 1.01 2.4391 9 2 2 4 37.13 1.69 2.4216 5 1 3 4 37.23 2.62 2.4150 12 1 2 4 37.53 1.14 2.3967 8 3 1 4 37.95 2.24 2.3712 6 1 3 4 38.01 2.12 2.3675 15 1 1 4 38.15 1.44 2.3589 13 2 1 4 38.31 1.06 2.3496 2 3 2 4 38.40 47.76 2.3439 14 2 0 4 38.45 2.36 2.3414 10 3 0 4 38.58 6.49 2.3335 8 0 3 2 38.67 1.14 2.3283 3 3 2 4 38.78 1.70 2.3223 9 3 1 4 38.86 4.59 2.3175 16 0 1 2 39.07 3.44 2.3056 13 1 2 4 39.18 5.59 2.2994 4 3 2 4 39.97 5.46 2.2558 8 1 3 4 40.09 6.51 2.2491 14 2 1 4 40.13 1.53 2.2469 10 3 1 4 40.48 1.35 2.2286 15 2 0 4 40.66 16.27 2.2187 4 2 3 4 40.95 22.46 2.2040 0 4 0 2 41.13 6.12 2.1946 10 0 3 2 41.29 2.51 2.1867 5 2 3 4 41.57 1.22 2.1726 3 4 0 4 42.04 2.21 2.1494 6 2 3 4 42.50 1.06 2.1270 17 1 1 4 42.62 5.24 2.1214 1 4 1 4 42.94 5.42 2.1063 15 1 2 4 43.14 1.02 2.0971 12 3 1 4 43.23 1.79 2.0926 13 3 0 4 43.54 1.53 2.0784 18 0 1 2 43.64 2.32 2.0742 9 3 2 4 43.84 1.64 2.0651 11 1 3 4 43.90 6.92 2.0624 8 2 3 4 44.08 2.57 2.0544 12 0 3 2 44.15 2.80 2.0513 16 2 1 4 44.20 2.26 2.0490 5 4 1 4 44.80 1.46 2.0230 18 1 1 4 44.83 8.89 2.0216 14 2 2 4 44.97 2.83 2.0159 16 1 2 4 45.41 1.14 1.9972 0 0 4 1 45.66 2.31 1.9868 19 1 0 4 45.66 5.31 1.9867 2 0 4 2 45.74 2.02 1.9835 7 4 1 4 46.21 8.84 1.9646 10 2 3 4 46.48 1.41 1.9536 14 3 1 4 46.68 2.11 1.9457 8 4 1 4 46.90 1.93 1.9373 20 0 0 2 46.99 4.50 1.9336 4 3 3 4 47.09 5.98 1.9297 0 4 2 2 47.14 4.73 1.9281 19 1 1 4 47.15 1.03 1.9274 1 4 2 4 47.37 5.85 1.9189 14 0 3 2 47.55 9.74 1.9123 5 3 3 4 47.62 2.44 1.9097 4 1 4 4 47.65 1.71 1.9086 3 4 2 4 47.66 3.51 1.9081 6 0 4 2 48.01 4.42 1.8949 18 0 2 2 48.08 2.52 1.8926 4 4 2 4 48.22 3.00 1.8872 6 3 3 4 48.42 1.02 1.8799 18 2 1 4 48.57 2.00 1.8743 16 2 2 4 48.74 1.39 1.8684 11 4 0 4 48.89 14.91 1.8629 10 4 1 4 48.91 3.54 1.8621 12 2 3 4 49.15 2.40 1.8536 13 3 2 4 49.18 3.00 1.8526 18 1 2 4 49.36 2.46 1.8464 8 0 4 2 49.90 2.45 1.8274 8 3 3 4 50.11 1.44 1.8203 12 4 0 4 50.14 10.12 1.8192 0 2 4 2 50.50 1.31 1.8072 8 1 4 4 50.75 2.54 1.7989 14 3 2 4 50.90 1.13 1.7938 9 3 3 4 50.94 5.15 1.7927 8 4 2 4 51.08 2.81 1.7880 4 2 4 4 51.36 1.40 1.7789 19 1 2 4 51.48 2.11 1.7753 10 0 4 2 51.49 1.75 1.7747 9 1 4 4 51.61 1.10 1.7711 5 2 4 4 51.91 1.48 1.7615 21 1 1 4 51.93 4.14 1.7609 9 4 2 4 51.97 3.69 1.7594 14 2 3 4 52.09 1.25 1.7557 16 1 3 4 52.24 5.86 1.7511 6 2 4 4 52.43 7.14 1.7452 15 3 2 4 52.50 3.78 1.7431 20 0 2 2 52.57 5.64 1.7409 18 2 2 4 52.59 1.76 1.7403 10 1 4 4 52.77 1.09 1.7347 4 5 0 4 52.88 2.90 1.7314 20 2 1 4 52.92 1.00 1.7301 13 4 1 4 53.02 2.59 1.7271 22 1 0 4 53.21 1.30 1.7216 11 3 3 4 53.26 1.20 1.7201 1 5 1 4 53.26 2.99 1.7199 22 0 1 2 53.97 1.18 1.6991 17 1 3 4 53.98 2.22 1.6986 12 0 4 2 54.04 2.04 1.6969 18 3 1 4 54.06 2.38 1.6963 1 4 3 4 54.10 1.85 1.6952 4 5 1 4 54.18 1.41 1.6927 16 3 2 4 54.20 1.39 1.6924 11 4 2 4 54.23 1.78 1.6914 2 4 3 4 54.44 1.28 1.6853 14 4 1 4 54.50 1.39 1.6838 12 3 3 4 54.60 2.44 1.6808 5 5 1 4 54.65 1.22 1.6793 19 2 2 4 54.84 3.54 1.6740 18 0 3 2 54.90 2.48 1.6724 4 4 3 4 55.06 1.36 1.6679 12 1 4 4 55.21 1.14 1.6636 6 5 1 4 55.46 1.94 1.6568 8 5 0 4 55.91 1.02 1.6447 18 1 3 4 56.00 2.80 1.6421 6 4 3 4 56.09 3.70 1.6397 19 3 1 4 56.43 1.73 1.6305 13 1 4 4 56.52 1.12 1.6283 4 3 4 4 56.71 1.20 1.6233 7 4 3 4 56.74 1.24 1.6223 8 5 1 4 56.82 2.35 1.6203 23 1 1 4 56.85 2.79 1.6196 14 0 4 2 56.93 1.07 1.6175 20 3 0 4 57.15 2.27 1.6116 1 5 2 4 57.52 1.53 1.6023 8 4 3 4 57.66 2.23 1.5987 9 5 1 4 57.91 3.54 1.5924 19 1 3 4 58.21 1.88 1.5850 12 2 4 4 58.55 2.63 1.5765 4 0 5 2 58.73 3.62 1.5722 0 1 5 2 59.02 1.89 1.5650 6 5 2 4 59.09 1.27 1.5634 8 3 4 4 59.43 1.75 1.5552 15 1 4 4 59.43 2.18 1.5551 10 4 3 4 59.79 1.72 1.5469 11 5 1 4 59.82 1.59 1.5460 15 4 2 4 60.94 1.41 1.5202 14 2 4 4 60.99 1.57 1.5193 12 5 1 4 61.07 2.96 1.5174 8 0 5 2 61.30 1.79 1.5121 18 4 1 4 61.37 1.50 1.5107 22 3 0 4 61.89 1.41 1.4993 25 1 1 4 61.96 1.10 1.4977 2 2 5 4 62.34 4.20 1.4894 24 2 1 4 62.99 1.10 1.4757 2 4 4 4 63.59 1.98 1.4631 6 2 5 4 63.67 1.16 1.4615 23 3 0 4 63.75 1.24 1.4599 3 6 0 4 63.99 1.10 1.4551 20 4 0 4 64.37 1.98 1.4473 14 4 3 4 64.48 1.11 1.4451 26 1 1 4 64.61 1.41 1.4426 6 4 4 4 64.86 2.17 1.4376 23 3 1 4 64.89 1.61 1.4369 18 4 2 4 65.28 3.15 1.4293 4 6 1 4 65.82 1.36 1.4188 15 4 3 4 66.01 1.16 1.4154 8 4 4 4 66.79 4.89 1.4006 10 2 5 4 66.92 1.26 1.3982 7 6 1 4 67.28 2.50 1.3916 15 3 4 4 67.30 2.16 1.3913 9 5 3 4 68.66 1.88 1.3670 14 1 5 4 69.25 1.20 1.3567 11 5 3 4 69.30 1.84 1.3559 22 4 1 4 70.66 1.33 1.3331 18 4 3 4 70.76 1.05 1.3315 0 0 6 1 71.20 2.28 1.3243 25 1 3 4 72.33 1.08 1.3064 22 1 4 4 72.41 1.37 1.3051 14 4 4 4 72.57 1.33 1.3026 28 2 1 4 72.89 1.01 1.2978 14 6 0 4 73.92 1.63 1.2822 4 4 5 4 74.43 1.44 1.2746 0 2 6 2 75.86 1.87 1.2542 29 1 2 4 76.02 1.12 1.2519 14 3 5 4 76.08 1.01 1.2510 10 5 4 4 77.31 1.31 1.2343 14 6 2 4 78.47 1.77 1.2189 25 3 3 4 80.13 1.00 1.1977 10 7 0 4 81.25 1.69 1.1840 0 5 5 2 86.38 1.01 1.1264 5 7 3 4 88.80 1.03 1.1018 29 1 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.