As6 Ge2 Na10 Eisenmann B, Klein J, Somer M Zeitschrift fur Kristallographie 197 (1991) 265-266 Crystal structure of decasodium di-mue-arsenidobis(diarsenidosilicate) _cod_database_code 1008852 _database_code_amcsd 0016718 CELL PARAMETERS: 13.5310 7.5440 8.2980 90.000 90.200 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 847.037 Density (g/cm3): 3.233 MAX. ABS. INTENSITY / VOLUME**2: 10.73024783 RIR: 1.081 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.49 28.01 7.0848 -1 0 1 2 12.53 89.09 7.0627 1 0 1 2 13.09 15.73 6.7655 2 0 0 2 13.44 45.71 6.5891 1 1 0 4 15.88 58.55 5.5820 0 1 1 4 17.17 49.39 5.1644 -1 1 1 4 17.61 46.25 5.0367 2 1 0 4 20.65 12.82 4.3007 2 1 1 4 21.42 18.56 4.1490 0 0 2 2 22.40 58.58 3.9686 -3 0 1 2 22.47 41.09 3.9570 3 0 1 2 23.59 77.61 3.7720 0 2 0 2 24.49 65.69 3.6354 0 1 2 4 25.36 20.97 3.5122 -3 1 1 4 25.39 13.08 3.5082 1 1 2 4 25.42 30.85 3.5042 3 1 1 4 26.79 2.05 3.3272 1 2 1 4 29.18 3.46 3.0602 2 2 1 4 30.88 4.38 2.8960 -4 1 1 4 30.90 8.57 2.8935 3 2 0 4 31.56 52.89 2.8347 -3 1 2 4 31.66 53.48 2.8262 3 1 2 4 32.07 20.14 2.7910 0 2 2 4 32.76 100.00 2.7341 -3 2 1 4 32.80 76.15 2.7303 3 2 1 4 33.03 6.97 2.7118 -1 0 3 2 33.08 3.22 2.7081 1 0 3 2 34.14 1.70 2.6263 -4 0 2 2 34.26 6.22 2.6173 4 0 2 2 34.54 9.78 2.5969 0 1 3 4 34.80 9.18 2.5779 2 2 2 4 34.83 2.98 2.5755 -5 0 1 2 34.91 2.05 2.5702 5 0 1 2 35.21 8.71 2.5488 1 1 3 4 35.23 4.60 2.5473 5 1 0 4 36.22 14.58 2.4803 -4 1 2 4 36.34 11.51 2.4723 1 3 0 4 36.88 11.51 2.4373 -5 1 1 4 36.95 6.57 2.4329 5 1 1 4 37.04 4.71 2.4271 -2 1 3 4 37.12 3.79 2.4218 2 1 3 4 37.37 68.42 2.4066 0 3 1 4 37.87 1.22 2.3758 -3 2 2 4 37.95 3.45 2.3708 3 2 2 4 37.97 2.72 2.3698 -1 3 1 4 38.11 57.53 2.3616 -3 0 3 2 38.18 1.69 2.3571 2 3 0 4 38.23 61.05 2.3542 3 0 3 2 39.77 9.17 2.2667 2 3 1 4 39.98 87.29 2.2552 6 0 0 2 40.01 17.12 2.2537 -3 1 3 4 40.12 11.82 2.2474 3 1 3 4 40.44 2.84 2.2305 0 2 3 4 40.99 9.77 2.2018 -1 2 3 4 41.54 3.24 2.1740 -5 1 2 4 42.01 47.81 2.1505 0 3 2 4 42.02 3.85 2.1503 4 2 2 4 42.56 19.89 2.1241 -3 3 1 4 42.56 4.77 2.1240 5 2 1 4 42.58 10.12 2.1233 1 3 2 4 42.60 28.31 2.1224 3 3 1 4 43.23 3.83 2.0927 -6 1 1 4 43.31 3.53 2.0893 6 1 1 4 43.63 18.65 2.0745 0 0 4 2 43.88 3.20 2.0632 -4 1 3 4 44.03 2.25 2.0567 4 1 3 4 44.17 2.05 2.0505 -2 3 2 4 44.22 1.46 2.0484 2 3 2 4 45.31 21.72 2.0016 -3 2 3 4 45.41 22.42 1.9972 3 2 3 4 45.70 8.75 1.9853 -2 0 4 2 45.79 3.18 1.9814 2 0 4 2 45.84 1.05 1.9797 -1 1 4 4 45.87 2.39 1.9785 6 0 2 2 46.28 3.26 1.9619 -4 3 1 4 46.76 11.62 1.9425 -3 3 2 4 46.83 14.33 1.9398 3 3 2 4 46.89 4.93 1.9377 -5 0 3 2 46.94 15.56 1.9356 6 2 0 4 47.37 6.17 1.9190 -6 1 2 4 47.44 7.21 1.9164 2 1 4 4 47.51 5.00 1.9138 6 1 2 4 48.25 3.77 1.8860 0 4 0 2 48.31 3.69 1.8840 -7 0 1 2 48.39 4.66 1.8811 7 0 1 2 48.62 1.07 1.8725 7 1 0 4 48.67 9.00 1.8707 5 1 3 4 48.95 2.63 1.8607 0 3 3 4 49.46 3.29 1.8427 1 3 3 4 49.48 1.65 1.8421 5 3 0 4 49.89 1.72 1.8279 -7 1 1 4 49.97 1.77 1.8252 7 1 1 4 50.05 1.81 1.8225 -1 4 1 4 50.06 4.14 1.8222 1 4 1 4 50.19 9.06 1.8177 0 2 4 4 50.22 1.82 1.8167 2 4 0 4 50.23 3.81 1.8163 -4 3 2 4 50.32 2.73 1.8133 4 3 2 4 50.74 1.40 1.7993 -5 3 1 4 50.80 1.32 1.7974 5 3 1 4 50.87 4.67 1.7951 -2 3 3 4 50.93 3.64 1.7930 2 3 3 4 51.60 8.29 1.7712 -4 0 4 2 51.78 9.67 1.7657 4 0 4 2 52.06 3.42 1.7568 -2 2 4 4 52.14 2.01 1.7541 2 2 4 4 52.21 5.66 1.7521 6 2 2 4 52.60 3.27 1.7400 3 4 0 4 53.11 3.17 1.7243 -4 1 4 4 53.14 2.02 1.7236 -5 2 3 4 53.21 2.64 1.7215 -3 3 3 4 53.25 1.22 1.7203 7 2 0 4 53.28 5.03 1.7192 4 1 4 4 53.30 1.04 1.7189 5 2 3 4 53.36 3.34 1.7169 0 4 2 4 53.75 2.70 1.7055 -6 1 3 4 53.78 1.42 1.7046 7 1 2 4 53.94 1.31 1.7000 6 1 3 4 54.23 2.41 1.6914 8 0 0 2 54.44 1.30 1.6855 -7 2 1 4 54.45 7.36 1.6851 -5 3 2 4 54.51 1.83 1.6834 7 2 1 4 55.17 1.31 1.6648 -2 4 2 4 55.21 11.47 1.6636 2 4 2 4 55.69 10.35 1.6504 8 1 0 4 55.78 1.34 1.6479 -1 0 5 2 55.81 1.41 1.6473 4 4 0 4 55.84 4.20 1.6466 1 0 5 2 55.84 18.15 1.6464 -6 3 1 4 55.90 13.14 1.6447 6 3 1 4 56.38 4.31 1.6319 -4 3 3 4 56.50 4.80 1.6287 4 3 3 4 56.80 5.78 1.6208 0 1 5 4 56.98 1.77 1.6163 -4 4 1 4 57.22 6.36 1.6100 -1 1 5 4 57.48 6.62 1.6032 -4 2 4 4 57.60 1.41 1.6002 0 3 4 4 57.64 4.82 1.5992 4 2 4 4 58.02 1.34 1.5897 -1 3 4 4 58.08 1.17 1.5881 -6 2 3 4 58.12 1.05 1.5870 -7 0 3 2 58.26 1.18 1.5836 6 2 3 4 58.51 1.24 1.5774 -2 1 5 4 59.26 1.85 1.5593 -3 0 5 2 59.33 13.83 1.5577 -6 3 2 4 59.38 3.72 1.5563 2 3 4 4 59.41 2.24 1.5557 3 0 5 2 59.44 9.70 1.5549 6 3 2 4 59.52 1.10 1.5530 -7 1 3 4 59.72 6.70 1.5484 -1 4 3 4 59.73 5.40 1.5482 7 1 3 4 59.77 1.08 1.5473 5 4 0 4 59.94 1.91 1.5433 8 2 0 4 60.40 3.22 1.5325 7 3 0 4 60.43 4.12 1.5319 -4 4 2 4 60.44 2.70 1.5317 8 1 2 4 60.54 5.67 1.5294 -6 0 4 2 60.77 4.05 1.5241 6 0 4 2 60.88 4.91 1.5216 -5 4 1 4 60.93 5.52 1.5205 5 4 1 4 60.99 2.08 1.5191 0 2 5 4 61.11 2.26 1.5164 8 2 1 4 61.43 14.32 1.5094 -3 3 4 4 61.44 4.58 1.5090 1 2 5 4 61.54 12.31 1.5069 3 3 4 4 62.57 1.49 1.4845 0 5 1 4 62.77 2.31 1.4803 -9 0 1 2 62.99 1.13 1.4757 -1 5 1 4 63.61 2.76 1.4628 -7 2 3 4 64.33 1.29 1.4481 -4 3 4 4 64.34 2.28 1.4480 -8 2 2 4 64.40 1.53 1.4467 6 4 0 4 64.49 3.21 1.4450 8 2 2 4 64.92 1.25 1.4363 7 3 2 4 65.06 1.48 1.4336 6 3 3 4 65.87 7.25 1.4180 0 5 2 4 65.90 3.39 1.4173 -6 2 4 4 66.12 2.04 1.4131 6 2 4 4 66.27 6.50 1.4103 -3 5 1 4 66.30 10.35 1.4098 3 5 1 4 66.64 1.70 1.4034 8 3 0 4 67.01 1.09 1.3966 9 2 0 4 67.07 1.67 1.3955 0 4 4 4 67.32 3.10 1.3908 -9 1 2 4 67.49 3.29 1.3878 9 1 2 4 67.49 1.39 1.3878 1 4 4 4 67.64 2.87 1.3851 0 3 5 4 67.69 1.01 1.3841 4 2 5 4 67.75 2.14 1.3831 8 3 1 4 67.76 2.15 1.3830 0 0 6 2 68.02 4.61 1.3783 -1 3 5 4 68.04 7.07 1.3780 -9 2 1 4 68.12 3.22 1.3765 9 2 1 4 68.66 3.74 1.3670 -6 4 2 4 69.04 1.71 1.3603 0 1 6 4 69.19 2.78 1.3578 -2 3 5 4 69.46 3.73 1.3531 -3 5 2 4 69.52 4.16 1.3522 3 5 2 4 69.69 2.99 1.3492 5 4 3 4 70.12 1.34 1.3421 -7 3 3 4 70.31 2.49 1.3390 7 3 3 4 70.57 1.23 1.3345 -2 1 6 4 70.71 1.11 1.3323 3 4 4 4 71.15 2.85 1.3252 -3 3 5 4 71.28 2.30 1.3230 3 3 5 4 71.29 3.60 1.3229 -9 0 3 2 71.32 1.08 1.3223 9 2 2 4 71.53 4.51 1.3190 9 0 3 2 71.58 1.89 1.3183 -6 1 5 4 71.84 2.20 1.3140 6 1 5 4 71.90 1.31 1.3131 -8 0 4 2 72.55 2.32 1.3030 -9 1 3 4 72.79 1.27 1.2993 9 1 3 4 72.84 3.35 1.2985 0 2 6 4 73.44 1.72 1.2894 8 1 4 4 73.88 1.12 1.2828 7 4 2 4 74.03 1.45 1.2805 4 3 5 4 74.44 3.21 1.2745 9 3 1 4 74.45 1.31 1.2744 2 2 6 4 74.65 1.93 1.2715 -3 5 3 4 74.79 2.16 1.2694 -10 1 2 4 75.19 2.18 1.2636 -4 1 6 4 75.35 1.39 1.2613 -7 0 5 2 75.40 3.97 1.2606 4 1 6 4 75.58 1.65 1.2580 6 2 5 4 75.66 2.19 1.2570 7 0 5 2 76.28 1.34 1.2483 -9 2 3 4 76.51 1.66 1.2451 9 2 3 4 76.58 4.34 1.2441 -7 1 5 4 76.65 2.59 1.2431 0 6 1 4 76.81 1.20 1.2410 -1 4 5 4 77.04 1.98 1.2379 1 6 1 4 77.38 1.15 1.2332 -9 3 2 4 77.51 1.24 1.2316 5 3 5 4 77.54 2.22 1.2311 9 3 2 4 78.17 1.19 1.2228 -2 6 1 4 78.37 1.94 1.2202 0 5 4 4 78.68 1.19 1.2162 11 0 1 2 78.82 1.81 1.2143 -7 4 3 4 78.88 1.22 1.2136 -4 2 6 4 79.07 3.73 1.2112 3 6 0 4 79.37 2.13 1.2073 -1 3 6 4 79.42 1.57 1.2067 1 3 6 4 79.49 1.69 1.2058 -8 4 2 4 79.62 4.47 1.2040 8 4 2 4 79.80 4.22 1.2019 -11 1 1 4 79.81 1.45 1.2017 -3 4 5 4 79.86 4.44 1.2010 -6 5 2 4 79.92 1.74 1.2004 2 5 4 4 79.97 2.01 1.1997 6 5 2 4 80.06 1.15 1.1986 -3 6 1 4 80.47 1.21 1.1935 -2 3 6 4 80.55 3.61 1.1925 7 2 5 4 80.93 1.46 1.1879 -6 4 4 4 81.21 5.25 1.1845 2 6 2 4 81.43 1.06 1.1818 -6 3 5 4 81.48 2.64 1.1813 -1 0 7 2 81.69 1.37 1.1787 6 3 5 4 82.34 1.06 1.1711 0 1 7 4 82.37 1.22 1.1707 -9 3 3 4 82.59 1.09 1.1681 4 4 5 4 82.72 1.29 1.1666 4 6 1 4 82.75 3.73 1.1663 1 1 7 4 83.23 1.11 1.1609 8 3 4 4 83.52 2.40 1.1575 11 2 1 4 84.68 3.02 1.1446 0 6 3 4 84.71 1.18 1.1443 10 3 2 4 84.92 2.49 1.1419 -4 3 6 4 85.04 2.25 1.1407 -1 6 3 4 85.13 2.61 1.1397 4 3 6 4 85.55 2.08 1.1351 -10 0 4 2 85.65 2.23 1.1341 -4 6 2 4 85.89 2.33 1.1315 10 0 4 2 85.98 2.08 1.1306 5 4 5 4 86.05 2.30 1.1299 -5 6 1 4 86.27 3.16 1.1276 12 0 0 2 86.28 2.41 1.1275 -7 3 5 4 86.30 2.52 1.1273 -1 2 7 4 86.47 1.81 1.1254 -11 0 3 2 86.64 1.02 1.1237 6 2 6 4 87.09 1.23 1.1190 10 1 4 4 87.35 1.18 1.1164 0 5 5 4 87.38 1.09 1.1160 -8 5 1 4 87.46 1.26 1.1153 0 4 6 4 87.70 2.64 1.1128 -1 5 5 4 87.95 3.95 1.1103 11 1 3 4 88.89 1.18 1.1009 -2 4 6 4 89.00 1.54 1.0999 2 4 6 4 89.28 3.12 1.0972 -9 3 4 4 89.43 1.38 1.0957 -11 3 1 4 89.45 1.01 1.0956 -10 3 3 4 89.58 1.85 1.0942 9 3 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.