Mcguinnessite Perchiazzi N Zeitschrift fur Kristallographie Supplement 23 (2006) 505-510 Crystal structure determination and Rietveld refinement of rosasite and mcguinnessite Locality: Red Mountain, California, USA _database_code_amcsd 0011133 CELL PARAMETERS: 12.9181 9.3923 3.1622 90.000 111.233 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 357.626 Density (g/cm3): 3.296 MAX. ABS. INTENSITY / VOLUME**2: 13.08268686 RIR: 1.292 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.95 10.07 7.4058 1 1 0 4 14.71 79.15 6.0206 2 0 0 2 17.50 9.82 5.0686 2 1 0 4 24.03 73.42 3.7029 2 2 0 4 24.11 23.17 3.6908 3 1 0 4 29.48 8.75 3.0300 1 3 0 4 29.68 2.41 3.0103 4 0 0 2 30.03 3.74 2.9758 -1 1 1 4 30.07 12.71 2.9721 -2 1 1 4 30.32 28.39 2.9475 0 0 1 2 31.20 3.35 2.8667 4 1 0 4 31.82 3.77 2.8123 0 1 1 4 31.93 5.34 2.8029 -3 1 1 4 34.00 4.01 2.6369 -4 0 1 2 34.38 1.80 2.6088 -1 2 1 4 34.41 100.00 2.6063 -2 2 1 4 35.19 3.89 2.5504 1 1 1 4 35.36 2.39 2.5387 -4 1 1 4 35.42 25.61 2.5343 4 2 0 4 35.97 35.05 2.4965 0 2 1 4 36.07 2.47 2.4899 -3 2 1 4 36.39 10.29 2.4686 3 3 0 4 38.33 3.51 2.3481 0 4 0 2 38.57 8.43 2.3344 2 0 1 2 38.60 10.35 2.3328 5 1 0 4 39.03 5.95 2.3079 1 2 1 4 39.18 6.87 2.2992 -4 2 1 4 40.00 2.15 2.2540 -5 1 1 4 40.71 1.52 2.2161 -1 3 1 4 40.74 5.82 2.2146 -2 3 1 4 41.27 13.98 2.1876 2 4 0 4 41.62 1.20 2.1699 4 3 0 4 42.10 11.79 2.1461 0 3 1 4 42.17 16.55 2.1429 5 2 0 4 44.47 2.69 2.0372 -6 0 1 2 44.81 2.49 2.0227 1 3 1 4 44.95 6.90 2.0168 -4 3 1 4 45.18 2.58 2.0069 6 0 0 2 45.32 9.19 2.0011 3 1 1 4 45.56 1.01 1.9909 -6 1 1 4 46.26 2.97 1.9626 6 1 0 4 47.64 13.12 1.9088 5 3 0 4 48.45 4.62 1.8790 -2 4 1 4 48.83 12.00 1.8650 -5 3 1 4 49.64 3.08 1.8366 0 4 1 4 49.72 1.06 1.8339 -3 4 1 4 50.92 3.83 1.7932 2 5 0 4 51.57 2.63 1.7721 4 1 1 4 51.84 7.76 1.7635 -7 1 1 4 52.16 17.62 1.7536 -4 4 1 4 53.46 3.95 1.7139 3 3 1 4 53.68 2.45 1.7075 -6 3 1 4 53.89 2.53 1.7014 3 5 0 4 54.21 8.13 1.6920 7 1 0 4 55.51 13.00 1.6555 2 4 1 4 55.67 1.61 1.6510 -5 4 1 4 57.82 1.08 1.5947 -8 0 1 2 58.24 2.40 1.5841 0 5 1 4 58.31 2.80 1.5824 -3 5 1 4 58.43 9.58 1.5794 5 1 1 4 58.87 6.00 1.5687 -2 0 2 2 58.96 6.11 1.5665 -4 0 2 2 59.01 1.75 1.5654 0 6 0 2 59.09 1.13 1.5634 4 3 1 4 59.33 7.04 1.5575 -7 3 1 4 59.86 7.08 1.5452 -4 1 2 4 59.93 1.59 1.5434 3 4 1 4 60.13 2.05 1.5388 -6 4 1 4 60.40 4.84 1.5325 1 5 1 4 61.12 2.03 1.5163 5 2 1 4 61.18 3.96 1.5150 2 6 0 4 61.40 1.15 1.5100 -8 2 1 4 61.51 5.82 1.5076 7 3 0 4 61.52 1.19 1.5074 -5 1 2 4 62.41 2.18 1.4879 -2 2 2 4 62.50 2.44 1.4860 -4 2 2 4 62.73 7.40 1.4812 5 5 0 4 63.73 3.91 1.4604 -5 5 1 4 63.82 1.24 1.4584 3 6 0 4 65.01 1.74 1.4347 6 0 1 2 65.08 1.78 1.4333 8 2 0 4 65.44 1.93 1.4263 5 3 1 4 66.17 7.64 1.4122 -9 1 1 4 66.49 3.72 1.4062 0 2 2 4 66.75 3.08 1.4015 -6 2 2 4 66.81 1.85 1.4003 -2 6 1 4 67.43 4.68 1.3888 4 6 0 4 67.68 2.60 1.3844 3 5 1 4 67.78 2.81 1.3825 0 6 1 4 67.84 2.02 1.3815 -7 1 2 4 67.87 1.79 1.3810 -6 5 1 4 70.64 1.39 1.3335 1 7 0 4 71.19 1.64 1.3245 9 1 0 4 72.46 3.26 1.3044 -2 4 2 4 72.54 1.31 1.3031 -4 4 2 4 73.85 2.70 1.2833 7 1 1 4 74.05 4.00 1.2802 1 3 2 4 74.37 1.06 1.2755 -7 3 2 4 74.57 2.59 1.2725 3 7 0 4 77.29 1.88 1.2344 3 1 2 4 77.60 1.92 1.2303 9 3 0 4 77.77 3.16 1.2281 -9 1 2 4 82.09 1.59 1.1740 0 8 0 2 83.56 1.08 1.1571 3 3 2 4 86.61 1.29 1.1240 1 5 2 4 86.77 2.14 1.1223 3 7 1 4 86.92 1.74 1.1208 -7 5 2 4 88.25 1.04 1.1073 -4 6 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.