Al Cl4 H4 N Mairesse G, Barbier P, Wignacourt J, Rubbens A, Wallart F Canadian Journal of Chemistry 56 (1978) 764-771 X-ray, Raman, infrared, and nuclear magnetic resonance studies of the crystal structure of ammonium tetrachloroaluminate, N H4 Al Cl4 _cod_database_code 1004065 _database_code_amcsd 0012165 CELL PARAMETERS: 11.0220 7.0720 9.2570 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 721.561 Density (g/cm3): 1.682 MAX. ABS. INTENSITY / VOLUME**2: 4.515162699 RIR: 0.874 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.49 10.23 7.0886 1 0 1 4 15.77 92.49 5.6197 0 1 1 4 16.08 17.86 5.5110 2 0 0 2 17.72 11.60 5.0065 1 1 1 8 18.74 84.92 4.7354 2 0 1 4 19.18 7.09 4.6285 0 0 2 2 20.43 4.43 4.3470 2 1 0 4 22.60 20.34 3.9347 2 1 1 8 24.36 75.29 3.6538 1 1 2 8 25.13 41.91 3.5443 2 0 2 4 25.19 13.19 3.5360 0 2 0 2 26.09 7.31 3.4149 3 0 1 4 28.16 20.59 3.1686 2 1 2 8 28.20 100.00 3.1642 1 2 1 8 29.04 47.47 3.0751 3 1 1 8 30.03 26.63 2.9761 2 2 0 4 30.07 25.79 2.9714 1 0 3 4 31.08 63.57 2.8776 3 0 2 4 31.58 46.61 2.8333 2 2 1 8 31.64 23.52 2.8282 0 1 3 4 31.85 31.98 2.8099 0 2 2 4 32.49 3.73 2.7555 4 0 0 2 32.69 7.02 2.7394 1 1 3 8 32.90 31.62 2.7228 1 2 2 8 33.28 10.62 2.6924 2 0 3 4 33.62 8.26 2.6654 3 1 2 8 33.94 39.93 2.6410 4 0 1 4 34.95 5.08 2.5675 4 1 0 4 35.68 6.38 2.5162 2 1 3 8 36.58 2.25 2.4564 3 2 1 8 38.00 2.08 2.3677 4 0 2 4 38.08 2.77 2.3629 3 0 3 4 38.92 1.14 2.3142 0 0 4 2 39.45 3.98 2.2844 0 3 1 4 39.62 39.02 2.2749 1 2 3 8 39.80 1.78 2.2649 1 0 4 4 40.16 15.57 2.2452 4 1 2 8 40.24 16.35 2.2411 3 1 3 8 40.32 1.70 2.2369 1 3 1 8 40.41 4.81 2.2319 3 2 2 8 41.55 1.03 2.1735 4 2 0 4 42.19 2.15 2.1421 2 2 3 8 42.36 1.48 2.1337 2 0 4 4 42.73 8.56 2.1159 4 2 1 8 42.85 1.47 2.1103 2 3 1 8 43.88 17.37 2.0634 1 3 2 8 44.06 11.60 2.0553 4 0 3 4 44.13 4.54 2.0522 5 1 1 8 46.21 7.80 1.9646 3 2 3 8 46.25 2.62 1.9628 2 3 2 8 46.83 7.15 1.9400 3 3 1 8 47.68 6.72 1.9072 1 2 4 8 48.22 2.47 1.8872 3 1 4 8 48.60 5.70 1.8732 0 3 3 4 49.63 13.39 1.8370 6 0 0 2 49.72 4.81 1.8336 5 2 1 8 49.95 3.49 1.8258 1 0 5 4 50.02 1.68 1.8236 3 3 2 8 50.66 3.02 1.8019 6 0 1 4 50.98 2.32 1.7913 4 3 0 4 50.99 4.77 1.7910 0 1 5 4 51.39 9.44 1.7780 6 1 0 4 51.42 5.47 1.7769 4 2 3 8 51.53 1.63 1.7736 2 3 3 8 51.70 24.59 1.7680 0 4 0 2 52.11 3.53 1.7550 2 0 5 4 52.40 7.46 1.7461 6 1 1 8 52.78 10.41 1.7344 5 2 2 8 53.49 59.51 1.7130 3 2 4 8 53.82 4.01 1.7033 2 1 5 8 54.51 1.06 1.6835 2 4 0 4 54.97 3.94 1.6705 4 3 2 8 55.03 9.01 1.6688 3 3 3 8 55.48 6.23 1.6563 2 4 1 8 56.74 4.70 1.6223 1 2 5 8 57.22 5.46 1.6099 3 1 5 8 57.62 15.79 1.5997 5 2 3 8 57.76 1.77 1.5962 5 0 4 4 58.15 2.19 1.5863 5 3 1 8 58.32 5.46 1.5821 2 4 2 8 58.47 1.29 1.5785 6 0 3 4 58.73 1.47 1.5720 2 2 5 8 59.96 1.26 1.5428 0 0 6 2 60.06 1.33 1.5405 6 1 3 8 60.18 5.47 1.5376 6 2 2 8 60.22 9.01 1.5367 4 0 5 4 60.98 3.62 1.5194 1 4 3 8 61.56 10.66 1.5064 3 4 2 8 61.57 1.24 1.5063 3 3 4 8 61.96 1.44 1.4977 3 2 5 8 62.15 1.83 1.4935 1 1 6 8 62.28 1.91 1.4907 7 0 2 4 62.52 1.33 1.4857 2 0 6 4 62.89 2.38 1.4778 2 4 3 8 63.30 8.98 1.4692 4 4 1 8 63.81 3.54 1.4586 7 1 2 8 63.94 2.73 1.4560 0 3 5 4 64.00 3.16 1.4548 5 2 4 8 64.04 4.10 1.4540 2 1 6 8 64.29 3.86 1.4490 6 3 0 4 64.67 2.43 1.4414 6 2 3 8 65.17 2.07 1.4316 6 3 1 8 65.63 1.08 1.4225 3 0 6 4 65.69 8.68 1.4213 7 2 1 8 65.88 1.18 1.4177 5 0 5 4 66.07 3.64 1.4141 0 2 6 4 66.41 1.41 1.4077 2 3 5 8 66.68 3.18 1.4026 1 2 6 8 66.69 2.47 1.4025 7 0 3 4 66.92 2.08 1.3982 0 5 1 4 68.05 1.96 1.3778 8 0 0 2 68.50 1.10 1.3697 2 2 6 8 68.90 1.02 1.3627 8 0 1 4 69.43 3.90 1.3536 3 3 5 8 70.09 1.54 1.3426 1 5 2 8 70.22 4.38 1.3403 4 4 3 8 71.32 1.53 1.3224 4 1 6 8 71.44 2.03 1.3205 8 0 2 4 71.73 1.04 1.3159 5 2 5 8 71.87 1.30 1.3137 2 5 2 8 71.91 1.15 1.3130 1 0 7 4 72.31 2.42 1.3067 3 5 1 8 72.50 4.29 1.3037 7 2 3 8 73.67 3.30 1.2859 2 0 7 4 73.68 1.03 1.2858 0 5 3 4 73.92 1.27 1.2822 1 3 6 8 74.48 6.40 1.2739 6 4 0 4 74.64 1.23 1.2716 8 2 1 8 74.74 1.47 1.2701 1 4 5 8 75.31 1.57 1.2620 6 4 1 8 75.45 2.88 1.2599 7 3 2 8 75.58 1.25 1.2581 4 2 6 8 75.66 1.52 1.2569 2 3 6 8 76.48 1.85 1.2455 2 4 5 8 77.56 1.05 1.2309 1 2 7 8 78.12 2.17 1.2235 6 2 5 8 78.82 2.20 1.2142 4 5 2 8 78.84 1.30 1.2141 9 0 1 4 80.57 2.50 1.1922 4 0 7 4 80.74 1.81 1.1902 5 2 6 8 81.19 1.01 1.1848 5 4 4 8 83.06 2.63 1.1627 1 6 1 8 83.31 5.95 1.1598 4 4 5 8 83.55 3.41 1.1571 0 0 8 2 84.76 1.22 1.1438 2 6 1 8 84.90 1.02 1.1422 0 6 2 4 85.13 1.33 1.1397 7 4 2 8 85.46 1.11 1.1361 1 6 2 8 85.48 2.52 1.1359 7 2 5 8 86.74 1.78 1.1227 9 2 2 8 86.93 1.72 1.1207 6 5 0 4 86.94 3.87 1.1205 6 2 6 8 87.72 1.96 1.1126 6 5 1 8 89.11 1.96 1.0988 7 4 3 8 89.44 2.54 1.0956 1 6 3 8 89.56 1.13 1.0945 10 0 1 4 89.58 1.56 1.0943 1 2 8 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.