Agricolaite Anderson A, Chieh C, Irish D E, Tong J P K Canadian Journal of Chemistry 58 (1980) 1651-1658 An X-ray crystallographic, Raman, and infrared spectral study of crystalline potassium uranyl carbonate, K4UO2(CO3)3 Locality: synthetic _database_code_amcsd 0012166 CELL PARAMETERS: 10.2470 9.2020 12.2260 90.000 95.110 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1148.243 Density (g/cm3): 3.508 MAX. ABS. INTENSITY / VOLUME**2: 35.55800855 RIR: 3.301 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.95 27.70 6.8343 1 1 0 4 14.48 100.00 6.1176 -1 1 1 4 14.55 52.16 6.0887 0 0 2 2 15.24 82.26 5.8137 1 1 1 4 17.38 49.02 5.1031 2 0 0 2 18.93 8.80 4.6872 -1 1 2 4 19.29 22.44 4.6010 0 2 0 2 20.10 1.94 4.4172 1 1 2 4 20.64 15.87 4.3040 0 2 1 4 21.70 19.56 4.0948 -2 0 2 2 23.73 38.33 3.7501 2 0 2 2 24.25 16.82 3.6708 0 2 2 4 24.83 17.54 3.5851 -1 1 3 4 26.08 12.16 3.4172 2 2 0 4 26.19 53.83 3.4020 1 1 3 4 26.67 3.93 3.3424 -2 2 1 4 27.53 41.65 3.2402 2 2 1 4 27.96 1.14 3.1910 3 1 0 4 28.31 38.40 3.1520 -3 1 1 4 29.20 9.33 3.0588 -2 2 2 4 29.34 7.88 3.0444 0 0 4 2 29.34 5.45 3.0439 0 2 3 4 29.53 15.25 3.0254 3 1 1 4 30.43 10.98 2.9375 1 3 0 4 31.14 7.07 2.8725 -1 3 1 4 31.45 2.04 2.8447 -1 1 4 4 31.51 3.59 2.8391 1 3 1 4 32.76 1.92 2.7340 3 1 2 4 32.89 29.41 2.7234 -2 0 4 2 33.25 6.91 2.6945 -2 2 3 4 33.53 45.23 2.6727 -1 3 2 4 34.23 5.56 2.6196 1 3 2 4 34.26 6.74 2.6171 -3 1 3 4 35.17 2.57 2.5516 4 0 0 2 35.33 2.91 2.5406 2 2 3 4 35.35 7.99 2.5389 0 2 4 4 35.66 1.38 2.5177 2 0 4 2 36.97 2.57 2.4318 -4 0 2 2 37.27 9.12 2.4126 3 1 3 4 37.32 6.64 2.4093 -1 3 3 4 38.28 1.96 2.3513 1 3 3 4 38.41 22.64 2.3436 -2 2 4 4 38.49 9.60 2.3387 -1 1 5 4 39.49 22.89 2.2819 4 0 2 2 39.56 3.76 2.2781 3 3 0 4 39.82 2.38 2.2638 -3 3 1 4 39.88 16.04 2.2605 0 4 1 4 40.04 3.38 2.2521 1 1 5 4 40.42 1.67 2.2314 4 2 0 4 40.53 2.63 2.2258 -4 2 1 4 40.86 3.16 2.2086 2 2 4 4 41.49 2.72 2.1767 -3 3 2 4 41.72 2.47 2.1652 4 2 1 4 41.97 16.54 2.1525 0 2 5 4 42.03 4.79 2.1499 -4 2 2 4 42.20 4.63 2.1415 -1 3 4 4 42.73 2.30 2.1162 3 1 4 4 43.22 1.53 2.0931 3 3 2 4 43.35 2.14 2.0873 1 3 4 4 43.52 4.34 2.0796 -2 4 1 4 44.08 22.73 2.0543 2 4 1 4 44.24 2.03 2.0474 -4 0 4 2 44.31 7.57 2.0443 4 2 2 4 44.37 5.69 2.0417 -2 2 5 4 44.43 1.43 2.0392 -3 3 3 4 44.65 1.38 2.0296 0 0 6 2 44.80 14.86 2.0231 -4 2 3 4 44.89 5.83 2.0191 -3 1 5 4 45.31 3.90 2.0014 0 4 3 4 45.48 4.24 1.9945 -5 1 1 4 45.52 1.80 1.9928 5 1 0 4 46.30 1.72 1.9609 2 4 2 4 46.67 2.00 1.9464 -2 0 6 2 46.83 3.60 1.9400 5 1 1 4 46.88 2.00 1.9379 3 3 3 4 47.10 2.05 1.9297 2 2 5 4 47.90 1.40 1.8990 -1 3 5 4 48.03 1.34 1.8941 4 2 3 4 48.10 5.43 1.8917 -2 4 3 4 48.46 6.43 1.8785 -3 3 4 4 48.55 5.88 1.8751 4 0 4 2 48.68 4.20 1.8705 -4 2 4 4 48.90 2.24 1.8624 3 1 5 4 49.06 3.80 1.8569 0 2 6 4 49.15 4.14 1.8538 -5 1 3 4 49.21 1.10 1.8517 1 3 5 4 49.65 3.38 1.8360 2 4 3 4 49.81 6.89 1.8307 2 0 6 2 50.38 5.97 1.8112 1 5 0 4 50.94 3.06 1.7926 -2 2 6 4 51.29 2.32 1.7812 -3 1 6 4 51.52 8.14 1.7739 3 3 4 4 52.48 6.57 1.7436 -1 5 2 4 52.91 3.24 1.7303 5 1 3 4 52.97 5.25 1.7286 1 5 2 4 53.41 2.21 1.7156 -3 3 5 4 53.49 1.01 1.7131 -4 2 5 4 53.58 6.68 1.7104 -1 1 7 4 53.73 2.35 1.7061 -4 4 1 4 53.90 2.26 1.7010 6 0 0 2 53.90 5.05 1.7010 2 2 6 4 53.92 1.15 1.7004 -5 3 1 4 53.96 6.70 1.6994 5 3 0 4 54.27 3.45 1.6902 -1 3 6 4 54.69 4.32 1.6783 4 4 1 4 54.72 4.73 1.6775 -6 0 2 2 54.90 6.98 1.6724 0 4 5 4 55.01 1.78 1.6692 -5 3 2 4 55.12 1.48 1.6662 5 3 1 4 55.26 3.00 1.6623 1 1 7 4 55.27 1.68 1.6621 -4 0 6 2 55.70 1.65 1.6501 1 3 6 4 56.56 1.73 1.6272 0 2 7 4 56.88 2.22 1.6188 -2 4 5 4 56.88 2.53 1.6187 3 5 0 4 56.97 1.25 1.6163 3 3 5 4 57.12 4.31 1.6126 -5 1 5 4 57.24 4.74 1.6095 -4 4 3 4 57.36 3.47 1.6063 5 3 2 4 57.54 2.34 1.6018 6 0 2 2 57.64 1.68 1.5993 -6 2 1 4 57.79 1.92 1.5955 6 2 0 4 58.04 1.18 1.5891 -2 2 7 4 58.25 1.46 1.5840 -3 1 7 4 58.36 2.36 1.5811 -3 5 2 4 58.57 5.01 1.5760 -6 2 2 4 58.92 2.00 1.5675 -1 5 4 4 59.10 1.24 1.5633 -4 2 6 4 59.13 5.42 1.5624 -3 3 6 4 59.18 2.21 1.5612 2 4 5 4 59.73 2.74 1.5482 3 5 2 4 59.83 1.50 1.5459 1 5 4 4 59.98 3.91 1.5422 4 4 3 4 60.35 2.08 1.5337 0 6 0 2 60.38 1.04 1.5330 -5 3 4 4 60.55 1.52 1.5290 -6 2 3 4 60.79 1.08 1.5236 4 0 6 2 60.88 2.56 1.5216 0 6 1 4 61.21 1.20 1.5142 2 2 7 4 61.28 1.61 1.5127 6 2 2 4 62.06 1.12 1.4956 -2 0 8 2 62.76 4.33 1.4805 5 1 5 4 62.95 1.64 1.4764 3 1 7 4 63.14 1.96 1.4724 3 3 6 4 63.99 1.37 1.4550 -3 5 4 4 64.05 1.12 1.4538 2 6 1 4 64.42 2.13 1.4464 4 2 6 4 64.49 1.27 1.4450 -7 1 1 4 64.52 2.74 1.4444 6 2 3 4 64.78 1.42 1.4391 5 3 4 4 65.16 1.38 1.4317 6 0 4 2 65.55 1.04 1.4242 -3 3 7 4 65.99 3.29 1.4157 7 1 1 4 66.57 2.95 1.4048 3 5 4 4 67.02 1.32 1.3965 -7 1 3 4 67.23 2.23 1.3926 -2 6 3 4 68.48 1.27 1.3701 -6 4 1 4 68.67 2.61 1.3669 5 5 0 4 68.85 1.44 1.3637 -2 4 7 4 68.94 1.59 1.3621 -1 5 6 4 68.96 2.72 1.3617 -4 0 8 2 69.00 1.15 1.3611 4 4 5 4 69.03 1.39 1.3606 2 2 8 4 69.73 1.16 1.3485 6 4 1 4 70.39 3.29 1.3376 1 3 8 4 70.46 2.09 1.3363 -2 6 4 4 71.15 1.41 1.3252 -6 4 3 4 71.29 2.29 1.3229 4 2 7 4 71.40 1.26 1.3211 7 1 3 4 71.66 1.46 1.3170 5 5 2 4 71.67 1.52 1.3168 7 3 0 4 71.75 1.07 1.3155 2 4 7 4 72.16 1.60 1.3090 -7 3 2 4 72.37 1.56 1.3057 -4 2 8 4 72.71 1.16 1.3005 4 6 1 4 72.89 1.18 1.2978 0 6 5 4 73.23 2.25 1.2925 -3 5 6 4 73.74 1.40 1.2849 -3 1 9 4 73.76 1.60 1.2845 -2 2 9 4 74.36 1.23 1.2757 -5 5 4 4 74.55 1.38 1.2729 4 6 2 4 74.59 2.20 1.2723 -2 6 5 4 74.82 3.35 1.2689 6 4 3 4 74.91 1.46 1.2677 -4 6 3 4 75.65 1.28 1.2570 -4 4 7 4 76.47 2.05 1.2457 -7 3 4 4 76.61 1.10 1.2437 2 6 5 4 77.08 1.32 1.2372 1 7 3 4 77.32 1.13 1.2341 4 6 3 4 77.34 1.75 1.2338 -8 2 1 4 77.46 1.24 1.2322 3 3 8 4 77.77 1.25 1.2281 -6 2 7 4 78.08 1.03 1.2240 -3 7 1 4 78.38 1.97 1.2201 5 5 4 4 78.55 1.46 1.2177 0 0 10 2 79.16 2.17 1.2099 3 1 9 4 80.40 1.04 1.1944 7 1 5 4 81.24 2.01 1.1842 4 4 7 4 81.95 1.15 1.1756 2 6 6 4 83.62 1.92 1.1564 -2 4 9 4 83.63 1.13 1.1563 1 5 8 4 85.01 1.07 1.1410 8 0 4 2 85.06 1.46 1.1404 -6 6 1 4 86.39 1.44 1.1263 -8 0 6 2 87.09 1.58 1.1190 -8 4 1 4 87.51 1.66 1.1147 -6 4 7 4 87.96 1.17 1.1102 -9 1 3 4 88.14 1.08 1.1083 2 6 7 4 89.46 1.07 1.0954 -7 5 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.