data_global
_amcsd_formula_title 'O14 P4 Pb V2'
loop_
_publ_author_name
'Boudin S'
'Grandin A'
'Leclaire A'
'Borel M'
'Raveau B'
_journal_name_full 'Journal of Materials Chemistry'
_journal_volume 4 
_journal_year 1994
_journal_page_first 1889
_journal_page_last 1892
_publ_section_title
;
 Two new diphosphates with SrV2(P2O7)2 structure: mercury and lead phases
 _cod_database_code 1001670
;
_database_code_amcsd 0013074
_chemical_formula_sum 'Pb V2 P4 O14'
_cell_length_a 4.804
_cell_length_b 7.113
_cell_length_c 7.898
_cell_angle_alpha 89.78
_cell_angle_beta 92.62
_cell_angle_gamma 106.10
_cell_volume 259.014
_exptl_crystal_density_diffrn      4.212
_symmetry_space_group_name_H-M 'P -1'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '-x,-y,-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Pb1   0.00000   0.00000   0.50000
V1   0.00000   0.00000   0.00000
V2   0.50000   0.50000   0.50000
P1   0.38170   0.77060   0.79780
P2   0.97280   0.38420   0.74900
O1   0.17800  -0.09560  -0.20470
O2  -0.08800   0.20230  -0.14740
O3  -0.37600  -0.17640  -0.07090
O4   0.12500   0.35140   0.58920
O5   0.70300   0.44570   0.70660
O6   0.47400   0.75650   0.61630
O7   0.19700   0.55670   0.85190