Fluorphosphohedyphane Miyake M, Ishigaki K, Suzuki T Journal of Solid State Chemistry 61 (1986) 230-235 Structure refinements of Pb2+ ion-exchanged apatites by X-ray powder pattern-fitting Note: Sample FAp Locality: synthetic Note: apatite group _database_code_amcsd 0013569 CELL PARAMETERS: 9.7590 9.7590 7.2910 90.000 90.000 120.000 SPACE GROUP: P6_3/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 601.351 Density (g/cm3): 5.332 MAX. ABS. INTENSITY / VOLUME**2: 65.60988858 RIR: 4.007 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.47 6.30 8.4515 1 0 0 6 18.18 7.02 4.8795 1 1 0 6 21.02 30.79 4.2258 2 0 0 6 21.92 27.44 4.0551 1 1 1 12 24.35 1.28 3.6561 2 0 1 12 24.42 12.07 3.6455 0 0 2 2 26.63 44.06 3.3474 1 0 2 12 27.93 14.37 3.1944 1 2 0 6 27.93 23.93 3.1944 2 1 0 6 30.55 36.15 2.9259 1 2 1 12 30.55 63.85 2.9259 2 1 1 12 30.61 89.67 2.9205 1 1 2 12 31.76 62.35 2.8172 3 0 0 6 32.44 6.36 2.7603 2 0 2 12 34.12 1.33 2.6278 3 0 1 12 36.84 2.54 2.4397 2 2 0 6 37.43 1.65 2.4025 2 1 2 12 38.40 1.23 2.3440 1 3 0 6 38.40 1.04 2.3440 3 1 0 6 40.47 4.59 2.2291 3 0 2 12 41.51 12.83 2.1754 1 1 3 12 42.80 4.69 2.1129 4 0 0 6 42.93 1.47 2.1068 2 0 3 12 44.69 32.14 2.0276 2 2 2 12 46.03 10.11 1.9716 1 3 2 12 46.03 11.18 1.9716 3 1 2 12 46.86 6.30 1.9389 2 3 0 6 46.86 2.29 1.9389 3 2 0 6 46.98 15.10 1.9342 1 2 3 12 46.98 12.73 1.9342 2 1 3 12 48.59 11.54 1.8738 2 3 1 12 48.59 10.01 1.8738 3 2 1 12 49.42 10.21 1.8443 1 4 0 6 49.42 11.11 1.8443 4 1 0 6 49.89 31.25 1.8280 4 0 2 12 50.04 14.30 1.8227 0 0 4 2 53.53 1.40 1.7119 3 2 2 12 53.68 1.26 1.7075 1 1 4 12 54.85 2.81 1.6737 2 0 4 12 55.87 1.46 1.6457 4 1 2 12 56.59 1.19 1.6265 3 3 0 6 57.72 4.10 1.5972 2 4 0 6 57.72 1.45 1.5972 4 2 0 6 58.11 5.08 1.5875 3 3 1 12 58.28 4.50 1.5831 1 2 4 12 58.28 3.70 1.5831 2 1 4 12 60.36 7.36 1.5335 5 0 2 12 60.50 11.37 1.5304 3 0 4 12 61.04 2.33 1.5179 5 1 0 6 61.15 1.70 1.5157 2 3 3 12 61.15 6.84 1.5157 3 2 3 12 62.50 2.31 1.4861 1 5 1 12 62.50 5.50 1.4861 5 1 1 12 62.53 6.43 1.4854 3 3 2 12 67.91 1.95 1.3801 4 0 4 12 69.55 1.86 1.3517 3 3 3 12 70.81 1.49 1.3306 2 5 1 12 70.81 2.36 1.3306 5 2 1 12 70.97 1.99 1.3280 2 3 4 12 71.06 4.71 1.3265 2 1 5 12 71.06 1.28 1.3265 1 2 5 12 71.85 4.18 1.3139 6 0 2 12 72.85 2.90 1.2983 3 4 2 12 72.85 1.25 1.2983 4 3 2 12 72.98 4.94 1.2964 1 4 4 12 72.98 4.50 1.2964 4 1 4 12 73.47 1.12 1.2888 1 6 0 6 73.47 1.07 1.2888 6 1 0 6 73.57 1.70 1.2875 1 5 3 12 73.57 2.01 1.2875 5 1 3 12 74.81 1.40 1.2692 1 6 1 12 74.81 1.05 1.2692 6 1 1 12 74.84 4.93 1.2687 2 5 2 12 74.84 3.20 1.2687 5 2 2 12 78.39 1.37 1.2199 4 4 0 6 79.72 1.06 1.2028 1 0 6 12 79.85 2.16 1.2013 2 4 4 12 79.85 1.63 1.2013 4 2 4 12 81.39 1.57 1.1824 5 2 3 12 81.66 3.68 1.1792 1 1 6 12 82.74 1.70 1.1664 5 1 4 12 82.83 2.42 1.1654 2 3 5 12 84.54 1.43 1.1461 7 0 2 12 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.