data_global _amcsd_formula_title 'K6.16Al6.16Ge9.84O32*4H2O' loop_ _publ_author_name 'Tripathi A' 'Parise J B' _journal_name_full 'Microporous and Mesoporous Materials' _journal_volume 52 _journal_year 2002 _journal_page_first 65 _journal_page_last 78 _publ_section_title ; Hydrothermal synthesis and structural characterization of the aluminogermanate analogues of JBW, montesommaite, analcime and paracelsian Sample: K-AlGe-MON ; _database_code_amcsd 0014407 _chemical_formula_sum 'K.77 (Al.77 Ge1.23) O4.5 H' _cell_length_a 7.373 _cell_length_b 7.373 _cell_length_c 17.513 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 952.027 _exptl_crystal_density_diffrn 2.975 _symmetry_space_group_name_H-M 'I -4 2 d' loop_ _space_group_symop_operation_xyz 'x,y,z' '1/2+x,1/2+y,1/2+z' '1/2-y,-x,3/4+z' '-y,1/2-x,1/4+z' 'y,-x,-z' '1/2+y,1/2-x,1/2-z' '-x,1/2+y,1/4-z' '1/2-x,+y,3/4-z' '-x,-y,z' '1/2-x,1/2-y,1/2+z' '1/2+y,x,3/4+z' '+y,1/2+x,1/4+z' '-y,x,-z' '1/2-y,1/2+x,1/2-z' 'x,1/2-y,1/4-z' '1/2+x,-y,3/4-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_U_iso_or_equiv K -0.01170 0.25000 0.12500 0.77000 0.10400 Al 0.47590 0.22310 0.03540 0.38500 0.01100 Ge 0.47590 0.22310 0.03540 0.61500 0.01100 O1 0.50000 0.00000 0.00670 1.00000 0.03300 O2 0.37740 0.25000 0.12500 1.00000 0.02200 O3 0.68690 0.32730 0.03260 1.00000 0.02300 Wat 0.00630 0.00090 0.00100 0.25000 0.01700 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 K 0.03000 0.19600 0.08400 0.00000 0.00000 0.09800 Al 0.01300 0.00900 0.01100 0.00000 0.00000 0.00100 Ge 0.01300 0.00900 0.01100 0.00000 0.00000 0.00100 O1 0.05400 0.01200 0.03500 0.00700 0.00000 0.00000 O2 0.01500 0.03800 0.01100 0.00000 0.00000 -0.00200 O3 0.01900 0.02900 0.02100 -0.00800 -0.00200 0.01100 Wat 0.00700 0.01300 0.03200 0.00800 0.01100 0.00900