Garavellite Bindi L, Menchetti S Mineralogy and Petrology 85 (2005) 131-139 Garavellite, FeSbBiS4, from the Caspari mine, North Rhine-Westphalia, Germany: composition, physical properties and determination of the crystal structure Locality: Caspari mine, North Rhine-Westphalia, Germany _database_code_amcsd 0014648 CELL PARAMETERS: 11.4130 14.1640 3.7590 90.000 90.000 90.000 SPACE GROUP: Pnam X-RAY WAVELENGTH: 1.541838 Cell Volume: 607.656 Density (g/cm3): 5.627 MAX. ABS. INTENSITY / VOLUME**2: 52.39689463 RIR: 3.032 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.95 72.07 8.8870 1 1 0 4 12.50 81.70 7.0820 0 2 0 2 14.72 10.65 6.0176 1 2 0 4 15.53 24.15 5.7065 2 0 0 2 16.75 5.63 5.2931 2 1 0 4 19.98 10.54 4.4435 2 2 0 4 20.36 12.33 4.3628 1 3 0 4 24.22 91.92 3.6741 3 1 0 4 24.47 47.55 3.6377 2 3 0 4 24.50 2.83 3.6332 0 1 1 4 25.15 9.39 3.5410 0 4 0 2 25.73 24.71 3.4620 1 1 1 8 26.35 12.44 3.3820 1 4 0 4 26.60 7.33 3.3514 3 2 0 4 27.99 99.41 3.1881 1 2 1 8 28.43 2.15 3.1391 2 0 1 4 29.14 30.19 3.0648 2 1 1 8 29.69 35.52 3.0088 2 4 0 4 30.40 11.68 2.9408 0 3 1 4 31.17 32.11 2.8698 2 2 1 8 31.41 2.12 2.8478 1 3 1 8 32.00 1.74 2.7971 4 1 0 4 32.57 12.75 2.7494 1 5 0 4 34.12 78.42 2.6275 3 1 1 8 34.30 100.00 2.6141 2 3 1 8 34.61 11.11 2.5920 3 4 0 4 35.38 28.46 2.5374 2 5 0 4 35.71 52.17 2.5142 1 4 1 8 36.81 9.71 2.4420 4 3 0 4 38.12 9.10 2.3607 0 6 0 2 38.32 9.11 2.3490 2 4 1 8 38.96 3.88 2.3117 1 6 0 4 39.66 11.64 2.2727 4 0 1 4 39.67 10.02 2.2721 3 5 0 4 40.01 2.24 2.2535 5 1 0 4 40.19 14.16 2.2440 4 1 1 8 40.61 2.30 2.2217 4 4 0 4 40.66 7.58 2.2191 1 5 1 8 41.39 20.09 2.1814 2 6 0 4 41.57 23.28 2.1725 5 2 0 4 41.74 20.56 2.1640 4 2 1 8 42.36 2.78 2.1339 3 4 1 8 43.01 1.21 2.1031 2 5 1 8 44.07 2.38 2.0550 5 3 0 4 44.23 27.53 2.0478 4 3 1 8 45.10 1.95 2.0103 4 5 0 4 45.20 5.23 2.0059 3 6 0 4 45.53 2.06 1.9924 1 7 0 4 46.71 6.94 1.9445 3 5 1 8 47.01 3.48 1.9328 5 1 1 8 47.38 29.11 1.9185 5 4 0 4 47.54 1.91 1.9126 4 4 1 8 47.82 1.51 1.9022 6 0 0 2 48.39 7.03 1.8810 5 2 1 8 48.43 31.95 1.8795 0 0 2 2 49.57 3.06 1.8388 1 1 2 8 50.16 1.05 1.8188 4 6 0 4 50.22 4.42 1.8166 0 2 2 4 50.62 11.55 1.8032 5 3 1 8 51.13 3.58 1.7865 3 7 0 4 51.17 2.36 1.7852 2 0 2 4 51.28 28.23 1.7817 0 7 1 4 51.41 1.06 1.7774 5 5 0 4 51.56 6.40 1.7727 4 5 1 8 51.62 1.95 1.7705 0 8 0 2 51.65 9.08 1.7697 3 6 1 8 51.82 1.25 1.7644 6 3 0 4 51.94 13.99 1.7604 1 7 1 8 52.89 1.42 1.7310 2 2 2 8 53.05 1.52 1.7261 1 3 2 8 53.91 4.13 1.7007 2 7 1 8 54.03 15.96 1.6972 6 0 1 4 54.87 16.78 1.6733 3 1 2 8 54.99 9.01 1.6698 2 3 2 8 55.34 1.99 1.6601 0 4 2 4 55.69 2.05 1.6505 4 7 0 4 55.69 1.53 1.6505 6 2 1 8 55.97 2.29 1.6428 1 4 2 8 56.10 1.77 1.6393 3 2 2 8 56.18 7.38 1.6373 4 6 1 8 56.84 3.59 1.6197 7 1 0 4 57.08 2.52 1.6135 3 7 1 8 57.34 10.87 1.6068 5 5 1 8 57.41 5.36 1.6052 3 8 0 4 57.72 1.58 1.5972 6 3 1 8 57.84 8.52 1.5941 2 4 2 8 58.05 9.43 1.5889 7 2 0 4 58.16 4.97 1.5862 1 8 1 8 59.27 3.42 1.5590 1 9 0 4 59.58 4.31 1.5516 1 5 2 8 60.49 3.29 1.5305 6 4 1 8 60.88 3.44 1.5216 3 4 2 8 61.39 8.91 1.5103 2 5 2 8 61.65 1.59 1.5044 4 8 0 4 62.34 3.60 1.4894 4 3 2 8 62.43 7.29 1.4875 7 1 1 8 62.96 8.21 1.4762 3 8 1 8 63.24 3.64 1.4704 0 6 2 4 63.83 1.49 1.4583 1 6 2 8 64.03 1.87 1.4543 3 9 0 4 64.15 3.68 1.4517 0 9 1 4 64.32 4.15 1.4482 3 5 2 8 64.99 1.01 1.4349 4 4 2 8 65.56 8.46 1.4239 2 6 2 8 65.69 10.11 1.4214 5 2 2 8 65.79 1.34 1.4194 8 1 0 4 66.46 4.58 1.4069 2 9 1 8 66.88 3.15 1.3990 5 8 0 4 67.59 4.42 1.3859 6 7 0 4 68.03 1.19 1.3781 4 9 0 4 68.03 7.23 1.3780 6 6 1 8 68.04 1.45 1.3779 7 4 1 8 68.22 3.61 1.3747 2 10 0 4 68.40 2.45 1.3715 3 6 2 8 68.65 1.05 1.3672 1 7 2 8 68.74 4.86 1.3656 8 3 0 4 70.09 14.70 1.3426 5 4 2 8 71.30 6.99 1.3227 7 5 1 8 71.68 1.25 1.3166 1 10 1 8 73.08 2.11 1.2949 3 7 2 8 73.14 1.65 1.2938 4 9 1 8 73.33 2.77 1.2911 2 10 1 8 73.48 1.09 1.2887 0 8 2 4 73.83 2.10 1.2836 8 3 1 8 74.10 3.48 1.2795 1 11 0 4 74.84 2.87 1.2687 4 10 0 4 75.20 1.41 1.2635 7 6 1 8 76.29 1.48 1.2482 8 4 1 8 76.87 1.41 1.2402 4 7 2 8 77.85 2.34 1.2270 7 1 2 8 77.87 4.00 1.2267 1 2 3 8 77.98 1.75 1.2252 6 8 1 8 78.00 2.42 1.2249 5 9 1 8 78.33 3.61 1.2206 3 8 2 8 78.43 1.27 1.2193 2 1 3 8 78.89 6.39 1.2134 7 2 2 8 78.96 1.05 1.2126 6 9 0 4 79.41 2.48 1.2067 8 5 1 8 79.47 1.24 1.2060 2 2 3 8 79.72 3.01 1.2028 7 7 1 8 79.78 1.72 1.2021 4 10 1 8 79.95 2.35 1.1999 1 9 2 8 80.00 1.95 1.1994 7 8 0 4 80.17 5.88 1.1973 9 1 1 8 81.09 4.34 1.1859 3 1 3 8 81.19 5.75 1.1847 2 3 3 8 81.20 1.40 1.1846 9 2 1 8 82.01 3.42 1.1750 1 4 3 8 82.05 1.16 1.1745 4 8 2 8 83.29 3.17 1.1601 3 11 1 8 84.18 1.37 1.1502 3 9 2 8 84.44 1.04 1.1472 4 0 3 4 84.78 1.12 1.1435 4 1 3 8 84.98 1.03 1.1413 10 0 0 2 85.78 1.12 1.1327 8 1 2 8 85.80 1.71 1.1325 4 2 3 8 86.34 1.40 1.1268 10 2 0 4 86.78 2.68 1.1222 5 8 2 8 87.44 3.74 1.1155 6 7 2 8 87.50 2.74 1.1148 4 3 3 8 87.85 1.04 1.1113 4 9 2 8 88.02 3.13 1.1096 2 10 2 8 88.36 3.08 1.1062 9 5 1 8 88.50 1.87 1.1048 2 12 1 8 88.50 4.25 1.1048 8 3 2 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.