Francoanellite Dick S, Zeiske T Zeitschrift fur Naturforschung B53 (1998) 711-719 Francoanellit K3Al5(HPO4)6(PO4)2*12H2O: struktur und synthese durch topochemische entwasserung von taranakit Locality: synthetic _database_code_amcsd 0015844 CELL PARAMETERS: 8.6900 8.6900 82.2700 90.000 90.000 120.000 SPACE GROUP: R-3c X-RAY WAVELENGTH: 1.541838 Cell Volume: 5380.364 Density (g/cm3): 2.285 MAX. ABS. INTENSITY / VOLUME**2: 7.267434939 RIR: 1.036 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.45 100.00 13.7117 0 0 6 2 11.95 55.72 7.4029 0 1 2 6 12.52 6.76 7.0675 1 0 4 6 12.91 23.44 6.8558 0 0 12 2 14.59 10.19 6.0732 0 1 8 6 15.96 39.50 5.5529 1 0 10 6 20.44 20.44 4.3450 1 1 0 6 20.70 22.39 4.2915 1 1 3 12 20.92 3.70 4.2456 1 0 16 6 21.45 35.67 4.1420 1 1 6 12 22.66 1.49 3.9242 1 1 9 12 24.04 2.60 3.7014 0 2 4 6 24.25 17.59 3.6700 1 1 12 12 24.66 5.99 3.6095 0 1 20 6 25.20 8.83 3.5337 2 0 8 6 25.99 11.18 3.4279 0 0 24 2 26.04 1.61 3.4219 0 2 10 6 26.17 64.13 3.4058 1 1 15 12 26.62 2.15 3.3489 1 0 22 6 28.16 17.57 3.1689 2 0 14 6 28.34 20.99 3.1491 1 1 18 12 29.41 26.18 3.0366 0 2 16 6 30.65 1.85 2.9169 0 1 26 6 30.73 37.36 2.9096 1 1 21 12 31.47 6.59 2.8428 2 1 1 12 31.76 2.02 2.8177 2 1 4 12 31.93 24.44 2.8029 1 2 5 12 32.24 23.39 2.7765 2 0 20 6 32.38 8.10 2.7647 2 1 7 12 32.65 4.76 2.7423 0 0 30 2 33.33 10.94 2.6883 2 1 10 12 33.71 11.42 2.6587 1 2 11 12 33.79 5.03 2.6525 0 2 22 6 35.05 4.69 2.5603 1 2 14 12 35.79 1.15 2.5086 3 0 0 6 36.00 2.87 2.4947 1 1 27 12 36.09 1.78 2.4890 2 1 16 12 36.41 1.32 2.4676 0 3 6 6 36.41 4.84 2.4676 3 0 6 6 37.12 1.65 2.4218 2 0 26 6 38.20 10.15 2.3558 0 3 12 6 38.20 1.09 2.3558 3 0 12 6 38.48 1.46 2.3396 1 2 20 12 39.10 6.37 2.3036 1 0 34 6 39.43 1.70 2.2853 0 0 36 2 39.82 1.83 2.2640 2 1 22 12 40.52 12.76 2.2263 1 2 23 12 41.71 3.21 2.1657 2 2 3 12 42.75 4.08 2.1154 1 2 26 12 43.36 13.42 2.0866 1 3 1 12 43.58 1.10 2.0766 1 3 4 12 44.06 7.22 2.0551 1 3 7 12 44.52 1.11 2.0352 0 2 34 6 44.77 6.10 2.0244 3 0 24 6 44.80 3.30 2.0232 1 3 10 12 44.81 2.12 2.0226 1 1 36 12 44.88 1.27 2.0198 2 2 15 12 45.10 6.18 2.0104 3 1 11 12 45.73 1.89 1.9840 1 0 40 6 46.27 3.76 1.9621 2 2 18 12 46.35 3.06 1.9588 0 0 42 2 47.68 1.03 1.9073 1 2 32 12 48.51 4.50 1.8766 2 0 38 6 49.45 3.67 1.8431 2 1 34 12 49.68 1.84 1.8350 2 2 24 12 49.71 1.56 1.8341 4 0 10 6 50.05 4.41 1.8226 1 3 22 12 50.36 2.10 1.8120 1 2 35 12 50.97 1.70 1.7918 0 4 14 6 51.15 3.76 1.7857 1 1 42 12 51.67 1.07 1.7689 2 2 27 12 52.22 4.10 1.7518 2 1 37 12 53.17 8.00 1.7228 1 2 38 12 53.66 1.63 1.7082 3 2 7 12 53.84 2.18 1.7027 2 3 8 12 53.88 1.74 1.7016 1 3 28 12 54.30 3.16 1.6894 0 3 36 6 54.55 1.21 1.6823 2 3 11 12 54.59 4.08 1.6812 3 1 29 12 55.47 2.55 1.6565 2 3 14 12 55.99 10.13 1.6423 4 1 0 12 56.05 1.71 1.6406 1 3 31 12 56.20 1.82 1.6367 3 2 16 12 56.43 1.10 1.6306 4 1 6 12 56.97 1.46 1.6164 4 1 9 12 57.72 1.12 1.5971 1 4 12 12 57.72 3.51 1.5971 4 1 12 12 57.93 2.83 1.5920 2 3 20 12 58.10 1.10 1.5875 2 1 43 12 58.39 2.22 1.5805 1 3 34 12 58.68 1.74 1.5732 4 1 15 12 59.20 1.16 1.5607 3 1 35 12 59.45 3.17 1.5549 2 3 23 12 59.73 1.11 1.5483 1 0 52 6 60.87 1.39 1.5218 1 3 37 12 61.30 1.07 1.5123 1 1 51 12 61.73 3.91 1.5027 3 1 38 12 62.38 1.43 1.4886 3 2 28 12 62.54 1.70 1.4853 4 0 34 6 64.37 1.32 1.4472 3 2 31 12 64.41 1.33 1.4466 3 1 41 12 64.45 1.19 1.4457 1 4 27 12 65.76 3.13 1.4201 0 4 38 6 66.01 1.21 1.4152 0 3 48 6 66.10 1.56 1.4135 5 0 20 6 66.27 2.10 1.4104 1 3 43 12 66.53 1.18 1.4054 3 2 34 12 66.75 2.20 1.4014 2 4 10 12 66.89 1.20 1.3988 2 2 45 12 67.47 1.28 1.3882 4 0 40 6 67.50 1.56 1.3876 2 4 13 12 67.89 1.06 1.3807 3 3 18 12 68.50 2.92 1.3697 1 1 57 12 68.57 1.19 1.3685 2 0 56 6 69.91 1.14 1.3456 2 2 48 12 70.27 1.09 1.3396 0 5 28 6 71.02 3.31 1.3273 0 2 58 6 72.40 1.20 1.3053 1 2 56 12 73.25 1.02 1.2922 3 1 50 12 73.79 1.77 1.2841 1 5 20 12 74.65 1.01 1.2714 4 2 29 12 75.85 1.28 1.2543 6 0 0 6 76.22 1.99 1.2491 0 6 6 6 76.35 1.47 1.2474 2 2 54 12 77.34 1.13 1.2338 0 6 12 6 78.49 1.38 1.2186 2 1 61 12 78.65 1.07 1.2164 0 2 64 6 79.54 1.35 1.2051 5 2 0 12 81.58 1.07 1.1800 5 1 34 12 82.90 1.16 1.1646 3 3 42 12 84.86 1.52 1.1426 0 0 72 2 87.10 1.14 1.1189 2 3 56 12 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.