Mo3 O14 P2 Sr Borel M, Guesdon A, Leclaire A, Grandin A, Raveau B Zeitschrift fur Anorganische und Allgemeine Chemie 620 (1994) 569-573 New mixed-valent molybdenum monophosphates with the KMo3P2O14 structure _cod_database_code 1001599 _database_code_amcsd 0015809 CELL PARAMETERS: 8.2880 6.4300 10.6480 90.000 112.830 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 522.997 Density (g/cm3): 4.199 MAX. ABS. INTENSITY / VOLUME**2: 29.77739322 RIR: 2.309 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.58 2.32 7.6387 1 0 0 2 11.60 8.35 7.6317 -1 0 1 2 16.48 15.31 5.3784 0 1 1 4 17.26 10.81 5.1385 1 0 1 2 17.28 4.52 5.1321 -1 0 2 2 18.03 3.86 4.9192 1 1 0 4 18.08 1.04 4.9069 0 0 2 2 21.44 8.12 4.1440 -2 0 1 2 22.14 46.61 4.0142 1 1 1 4 22.16 6.35 4.0111 -1 1 2 4 22.80 17.88 3.9008 0 1 2 4 23.29 28.53 3.8194 2 0 0 2 23.31 5.40 3.8158 -2 0 2 2 25.09 4.53 3.5495 1 0 2 2 25.11 1.34 3.5460 -1 0 3 2 25.57 73.66 3.4833 -2 1 1 4 27.16 28.41 3.2837 2 1 0 4 27.17 9.96 3.2815 -2 1 2 4 27.26 44.13 3.2713 0 0 3 2 27.75 100.00 3.2150 0 2 0 2 28.20 46.73 3.1640 -2 0 3 2 28.73 1.88 3.1075 1 1 2 4 28.75 4.14 3.1051 -1 1 3 4 30.66 29.77 2.9156 0 1 3 4 31.48 15.80 2.8418 2 1 1 4 31.51 7.97 2.8389 -2 1 3 4 32.86 3.73 2.7255 1 2 1 4 33.73 4.38 2.6571 1 0 3 2 34.92 4.28 2.5693 2 0 2 2 34.97 2.44 2.5661 -2 0 4 2 35.25 5.23 2.5462 3 0 0 2 35.28 2.93 2.5439 -3 0 3 2 35.33 7.26 2.5402 -2 2 1 4 35.66 1.61 2.5177 -3 1 1 4 36.55 1.43 2.4587 -2 2 2 4 36.59 2.91 2.4557 1 1 3 4 36.62 2.14 2.4541 -1 1 4 4 37.70 1.33 2.3859 2 1 2 4 37.75 6.93 2.3833 -2 1 4 4 37.75 6.32 2.3828 1 2 2 4 38.01 6.82 2.3674 3 1 0 4 39.29 9.07 2.2930 0 2 3 4 39.30 1.32 2.2923 0 1 4 4 39.93 8.52 2.2579 -3 0 4 2 39.98 13.66 2.2551 -2 2 3 4 42.43 2.92 2.1304 -3 1 4 4 42.81 8.19 2.1124 2 0 3 2 42.87 12.03 2.1097 1 0 4 2 42.89 1.07 2.1084 -1 0 5 2 43.20 2.39 2.0940 0 3 1 4 43.44 2.48 2.0833 -3 2 2 4 43.69 1.34 2.0720 -4 0 2 2 43.87 4.56 2.0636 1 3 0 4 44.22 2.89 2.0481 1 2 3 4 44.24 2.30 2.0472 -1 2 4 4 44.69 2.09 2.0278 -4 0 1 2 44.71 9.13 2.0268 -4 0 3 2 45.18 5.81 2.0071 2 2 2 4 45.21 1.04 2.0056 -2 2 4 4 45.24 4.49 2.0046 1 1 4 4 45.44 5.72 1.9961 3 2 0 4 45.47 4.15 1.9949 -3 2 3 4 45.87 7.34 1.9781 1 3 1 4 46.22 2.14 1.9641 0 3 2 4 47.62 4.44 1.9097 4 0 0 2 47.66 2.38 1.9079 -4 0 4 2 47.78 15.54 1.9038 -2 3 1 4 48.40 1.91 1.8807 -3 1 5 4 48.49 5.59 1.8773 0 1 5 4 48.72 4.33 1.8691 2 3 0 4 48.73 1.48 1.8687 -2 3 2 4 49.32 2.23 1.8477 -3 2 4 4 49.70 3.71 1.8343 -1 3 3 4 49.81 4.10 1.8306 4 1 0 4 49.86 7.50 1.8291 -4 1 4 4 50.94 5.85 1.7928 0 3 3 4 51.48 4.34 1.7752 2 3 1 4 51.50 1.80 1.7745 -2 3 3 4 51.55 10.86 1.7730 -2 0 6 2 51.78 1.78 1.7654 2 2 3 4 51.83 8.84 1.7639 1 2 4 4 52.55 2.87 1.7416 -4 2 2 4 53.42 3.84 1.7152 -4 2 1 4 53.44 5.02 1.7145 -4 2 3 4 53.62 1.11 1.7092 -2 1 6 4 54.35 2.67 1.6880 -4 1 5 4 55.05 2.87 1.6682 1 3 3 4 55.52 16.91 1.6551 3 1 3 4 55.89 4.78 1.6450 -2 3 4 4 56.01 1.03 1.6419 4 2 0 4 56.05 4.09 1.6408 -4 2 4 4 56.09 5.58 1.6397 3 3 0 4 57.06 1.49 1.6141 0 3 4 4 57.32 13.73 1.6075 0 4 0 2 57.32 2.67 1.6073 -5 0 1 2 57.61 1.43 1.5999 -5 1 2 4 57.62 8.03 1.5996 -5 1 3 4 58.20 3.11 1.5852 0 1 6 4 58.33 2.43 1.5820 -4 0 6 2 59.54 10.61 1.5525 -2 2 6 4 61.69 1.81 1.5035 1 3 4 4 62.48 4.90 1.4864 5 1 0 4 62.55 2.15 1.4850 -1 0 7 2 62.71 1.26 1.4816 2 4 0 4 64.36 4.61 1.4476 1 1 6 4 64.36 1.23 1.4475 0 3 5 4 64.39 3.29 1.4470 -1 1 7 4 64.60 3.97 1.4427 0 4 3 4 64.85 1.74 1.4377 -5 2 1 4 65.08 4.70 1.4331 -2 4 3 4 65.46 1.42 1.4258 4 3 0 4 65.50 4.92 1.4251 -4 3 4 4 65.79 2.79 1.4195 -4 2 6 4 67.24 1.63 1.3923 -5 1 6 4 67.35 4.94 1.3903 -4 1 7 4 68.90 1.12 1.3627 2 4 2 4 69.10 1.16 1.3593 3 4 0 4 69.62 1.12 1.3505 -6 1 3 4 69.76 1.16 1.3482 -1 2 7 4 70.36 10.08 1.3381 3 3 3 4 71.44 1.44 1.3205 5 0 2 2 72.21 4.94 1.3082 -5 3 3 4 72.51 1.54 1.3036 -5 2 6 4 72.72 1.29 1.3003 0 3 6 4 74.12 1.24 1.2792 2 4 3 4 74.16 2.46 1.2786 1 4 4 4 75.48 1.99 1.2595 -4 4 3 4 76.59 3.80 1.2441 5 3 0 4 76.86 1.15 1.2403 -2 3 7 4 77.69 1.13 1.2291 -6 2 1 4 77.76 2.02 1.2282 -2 5 1 4 78.27 2.11 1.2215 5 2 2 4 78.30 3.08 1.2210 1 3 6 4 78.33 1.72 1.2207 -1 3 7 4 80.20 1.38 1.1968 0 5 3 4 80.68 4.13 1.1909 -2 4 6 4 80.98 1.00 1.1873 -5 3 6 4 81.08 4.08 1.1861 -4 3 7 4 81.36 1.23 1.1827 -6 2 6 4 81.44 1.20 1.1818 -7 0 4 2 82.98 1.73 1.1636 3 1 6 4 83.59 1.40 1.1567 -2 1 9 4 86.27 1.13 1.1276 -4 4 6 4 88.55 1.02 1.1043 -2 2 9 4 89.87 1.02 1.0915 -4 2 9 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.